1CNV

CRYSTAL STRUCTURE OF CONCANAVALIN B AT 1.65 A RESOLUTION

Experimental procedure

Detector technology	IMAGE PLATE
Collection date	1993-12-13
Detector	MARRESEARCH
Spacegroup name	P 61
Unit cell lengths	81.400, 81.400, 102.200
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	10.000 - 1.650
R-factor	0.172
Rwork	0.172
RMSD bond length	0.008
RMSD bond angle	1.850
Data reduction software	XDS
Data scaling software	XDS
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	15.000
High resolution limit [Å]	1.650	1.650 *
Rmerge	0.004 *	0.230 *
Total number of observations	145907 *
Number of reflections	40387
Completeness [%]	85.9	64.1 *
Redundancy	3.9	2.9 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Microdialysis *