1CIV
CHLOROPLAST NADP-DEPENDENT MALATE DEHYDROGENASE FROM FLAVERIA BIDENTIS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM02 |
Synchrotron site | ESRF |
Beamline | BM02 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1996-09-01 |
Detector | RIGAKU |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 147.800, 147.800, 64.900 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 15.000 - 2.800 |
R-factor | 0.205 * |
Rwork | 0.205 |
R-free | 0.28400 |
Structure solution method | SIRAS |
Starting model (for MR) | 4mdh |
RMSD bond length | 0.009 |
RMSD bond angle | 1.740 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CCP4 |
Refinement software | X-PLOR (3.84) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.800 |
Rmerge | 0.132 |
Total number of observations | 38553 * |
Number of reflections | 20335 |
Completeness [%] | 98.3 |
Redundancy | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7.5 | 291 * | SEE MACPHERSON ET AL. (1998) ACTA CRYST, D54, 654 - 656, pH 7.50 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | ammonium sulfate | 1.5 (M) | |
2 | 1 | 1 | HEPES | 0.1 (M) | |
3 | 1 | 1 | glycerol | 12 (%) |