1CIC
IDIOTOPE-ANTI-IDIOTOPE FAB-FAB COMPLEX; D1.3-E225
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 293 |
Detector technology | AREA DETECTOR |
Collection date | 1987-11 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 75.110, 77.650, 96.750 |
Unit cell angles | 90.00, 111.80, 90.00 |
Refinement procedure
Resolution | 7.000 - 2.500 |
R-factor | 0.179 * |
Rwork | 0.179 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | FAB D1.3 |
RMSD bond length | 0.016 |
RMSD bond angle | 0.042 |
Data reduction software | ROTAVATA |
Data scaling software | CCP4 ((AGROVATA) |
Phasing software | AMoRE |
Refinement software | PROFFT |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 13.700 |
High resolution limit [Å] | 2.500 |
Rmerge | 0.076 |
Number of reflections | 33526 |
Completeness [%] | 97.0 |
Redundancy | 2.84 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.9 | 12% PEG 800, 75 MILLIMOLAR SODIUM ACETATE PH 4.85 10MGM/ML PROTEIN CONCENTRATION , pH 4.9 |