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1CH2

RECOMBINANT SPERM WHALE MYOGLOBIN L89F MUTANT (MET)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsSIEMENS
Temperature [K]295
Detector technologyIMAGE PLATE
Collection date1997-07-03
DetectorRIGAKU RAXIS IIC
Spacegroup nameP 6
Unit cell lengths91.431, 91.431, 45.909
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution5.000 - 1.800
R-factor0.1416
R-free0.15200

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Structure solution methodOTHER
Starting model (for MR)1MBW
RMSD bond length0.010
RMSD bond angle2.100

*

Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwareX-PLOR
Refinement softwareSHELXL-97
Data quality characteristics
 Overall
Low resolution limit [Å]50.000
High resolution limit [Å]1.800
Rmerge0.059
Total number of observations139450

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Number of reflections20451

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Completeness [%]99.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion, hanging drop

*

92.6-3.0 M (NH4)2SO4, 20 MM TRIS, 1 MM EDTA, PH 9.0
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein20 (mg/ml)
21dropammonium sulfate2.4-3.0 (M)
31dropTris-HCl20 (mM)
41dropEDTA1 (mM)
51reservoirammonium sulfate2.4-3.0 (M)

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