1CGN

CYTOCHROME C'

Experimental procedure

Detector technology	IMAGE PLATE
Collection date	1993-03-20
Detector	RIGAKU RAXIS IIC
Spacegroup name	P 65 2 2
Unit cell lengths	54.600, 54.600, 180.400
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	20.000 - 2.150
R-factor	0.167
RMSD bond length	0.013 *
RMSD bond angle	2.100 *
Data reduction software	SUPPLIED (SOFTWARE)
Refinement software	TNT (5C)

Data quality characteristics

	Overall
High resolution limit [Å]	2.150 *
Rmerge	0.032
Total number of observations	60526 *
Number of reflections	8220 *
Completeness [%]	90.0 *
Redundancy	7.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	6 *	37 *	Norris, G. E., (1979) J.Mol.Biol., 135, 309. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	12 (mg/ml)
2	1	drop	phosphate	0.1 (M)
3	1	drop	ammonium sulfate	50 (%sat)
4	1	reservoir	ammonium sulfate	62-66 (%sat)