1CFM
CYTOCHROME F FROM CHLAMYDOMONAS REINHARDTII
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1996-11 |
Detector | RIGAKU |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 75.624, 94.943, 119.920 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.000 - 2.000 |
R-factor | 0.214 |
Rwork | 0.214 |
R-free | 0.27100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ctm |
RMSD bond length | 0.006 |
RMSD bond angle | 24.300 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (0.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.600 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.042 * | 0.176 * |
Number of reflections | 47521 | |
<I/σ(I)> | 14.8 | 3.5 |
Completeness [%] | 91.6 * | 68.7 * |
Redundancy | 3.3 | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 6.5 | 4 * | pH 6.5 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG8000 | 180 (g/L) | |
2 | 1 | reservoir | sodium cacodylate | 0.1 (M) | |
3 | 1 | reservoir | 0.2 (M) |