1CDC

CD2, N-TERMINAL DOMAIN (1-99), TRUNCATED FORM

Experimental procedure

Source type	SYNCHROTRON
Source details	SRS BEAMLINE PX9.6
Synchrotron site	SRS
Beamline	PX9.6
Detector technology	IMAGE PLATE
Collection date	1994-05-22
Detector	MARRESEARCH
Spacegroup name	P 21 21 21
Unit cell lengths	55.900, 57.050, 60.560
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 2.000
R-factor	0.192
Rwork	0.192
RMSD bond length	0.013
RMSD bond angle	0.048 *
Data reduction software	DENZO
Phasing software	X-PLOR
Refinement software	PROLSQ

Data quality characteristics

	Overall
Low resolution limit [Å]	6.000
High resolution limit [Å]	2.000
Rmerge	0.065
Total number of observations	51353 *
Number of reflections	13465
Completeness [%]	99.3
Redundancy	3.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	7 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	ammonium sulfate	2.5 (M)