1CCK
ALTERING SUBSTRATE SPECIFICITY OF CYTOCHROME C PEROXIDASE TOWARDS A SMALL MOLECULAR SUBSTRATE PEROXIDASE BY SUBSTITUTING TYROSINE FOR PHE 202
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 290 |
Detector technology | AREA DETECTOR |
Collection date | 1995-06 |
Detector | SIEMENS |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 103.500, 73.400, 44.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 5.000 - 2.100 |
R-factor | 0.184 |
Rwork | 0.184 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1cca |
Data reduction software | XENGEN |
Data scaling software | XENGEN |
Phasing software | X-PLOR (3.1) |
Refinement software | XTALVIEW |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 2.090 | |
High resolution limit [Å] | 2.100 | 2.010 |
Rmerge | 0.070 | |
Number of reflections | 23157 | |
<I/σ(I)> | 7.1 | 1 |
Completeness [%] | 91.3 | 77.5 |
Redundancy | 2.2 | 1.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | DIALYSIS AGAINST DISTILLED WATER, dialaysis |