1CAX

DETERMINATION OF THREE CRYSTAL STRUCTURES OF CANAVALIN BY MOLECULAR REPLACEMENT

Experimental procedure

Spacegroup name	C 2 2 21
Unit cell lengths	136.500, 150.300, 133.400
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.600
R-factor	0.175
RMSD bond length	0.020
RMSD bond angle	2.987 *
Refinement software	TNT

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	2.600 *	2.600 *
Rmerge	0.055 *	0.174 *
Total number of observations	140046 *
Number of reflections	37938 *	7058 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	6.8 *