1CAW

DETERMINATION OF THREE CRYSTAL STRUCTURES OF CANAVALIN BY MOLECULAR REPLACEMENT

Experimental procedure

Spacegroup name	H 3
Unit cell lengths	136.800, 136.800, 75.700
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	8.000 - 2.600
R-factor	0.194
RMSD bond length	0.020
RMSD bond angle	2.911 *
Refinement software	TNT

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	2.500 *	2.500 *
Rmerge	0.064 *	0.151 *
Total number of observations	26041 *
Number of reflections	11525 *	2212 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	6.8 *