1C8F
FELINE PANLEUKOPENIA VIRUS EMPTY CAPSID STRUCTURE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F1 |
Synchrotron site | CHESS |
Beamline | F1 |
Temperature [K] | 277 |
Detector technology | OSCILLATION CAMERA |
Collection date | 1992-01-15 |
Wavelength(s) | 0.9, 1.4 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 380.120, 379.250, 350.820 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 9.000 - 3.000 |
R-factor | 0.285 |
Rwork | 0.285 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.589 |
Phasing software | GLRF |
Refinement software | CNS (0.5) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.800 | 3.200 |
High resolution limit [Å] | 2.700 | 3.000 |
Rmerge | 0.146 | |
Number of reflections | 547268 | |
<I/σ(I)> | 11.2 | |
Completeness [%] | 59.6 | 35 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 7.5 | 19 * | 0.75-1.5% PEG8000, 8 mM CaCl2, 20 mM Tris pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 294K |
1 | Vapor diffusion, sitting drop * | 7.5 | 19 * | 0.75-1.5% PEG8000, 8 mM CaCl2, 20 mM Tris pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 294K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | virus | 10 (mg/ml) | |
2 | 1 | drop | Bis-Tris | 20 (mM) | |
3 | 1 | drop | Tris-HCl | 20 (mM) | |
4 | 1 | reservoir | PEG8000 | 0.75-1.50 (%) | |
5 | 1 | reservoir | 8 (mM or 5 mM EDTA) |