1C7G
TYROSINE PHENOL-LYASE FROM ERWINIA HERBICOLA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | MACSCIENCE M18X |
Temperature [K] | 293 |
Detector technology | AREA DETECTOR |
Collection date | 1998-05-01 |
Detector | SIEMENS |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 163.490, 113.040, 101.090 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.100 |
R-factor | 0.1862 |
Rwork | 0.186 |
R-free | 0.24200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1tpl |
RMSD bond length | 0.007 |
RMSD bond angle | 1.442 |
Data reduction software | SAINT |
Data scaling software | SAINT |
Phasing software | X-PLOR |
Refinement software | X-PLOR (3.85) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.000 | 2.079 |
High resolution limit [Å] | 2.007 | 2.007 |
Number of reflections | 113432 | |
<I/σ(I)> | 1.34 | |
Completeness [%] | 90.3 | 53.7 |
Redundancy | 4.59 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.2 | 30% PEG6000, 0.2M AMMONIUM ACETATE, 0.1M SODIUM CITRATE, PH 6.2 |