1C58
CRYSTAL STRUCTURE OF CYCLOAMYLOSE 26
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE X31 |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | X31 |
| Temperature [K] | 277 |
| Detector technology | IMAGE PLATE |
| Collection date | 1998-01-01 |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 |
| Unit cell lengths | 21.840, 22.920, 29.050 |
| Unit cell angles | 87.36, 89.51, 61.98 |
Refinement procedure
| Resolution | 29.020 - 0.990 |
| R-factor | 0.082 * |
| R-free | 0.10000 |
| Structure solution method | DIRECT METHODS |
| Starting model (for MR) | MALTOSE DISACCHARIDE |
| Data scaling software | SCALEPACK |
| Phasing software | SHELXD |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.020 | 1.010 |
| High resolution limit [Å] | 0.990 | 0.990 |
| Rmerge | 0.037 | 0.190 * |
| Number of reflections | 26766 | |
| <I/σ(I)> | 18.07 | 6.94 |
| Completeness [%] | 96.7 | 84.1 |
| Redundancy | 2.79 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 37.5% PEG 400, VAPOR DIFFUSION |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | PEG400 | 37.5 (%(v/v)) |
