1C3P
CRYSTAL STRUCTURE OF AN HDAC HOMOLOG FROM AQUIFEX AEOLICUS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 103 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 51.400, 93.800, 78.700 |
Unit cell angles | 90.00, 96.90, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.800 |
R-factor | 0.198 |
Rwork | 0.198 |
R-free | 0.24000 |
RMSD bond length | 0.010 * |
RMSD bond angle | 1.630 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MLPHARE |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 1.800 |
Rmerge | 0.029 |
Total number of observations | 134952 * |
Number of reflections | 32143 * |
Completeness [%] | 92.3 * |
Redundancy | 4.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7 | PEG 1500, SODIUM CHLORIDE, ISOPROPANOL, TRIS-HCL, pH 7.00 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | isopropanol | 7.5 (%) | |
2 | 1 | reservoir | PEG1500 | 28 (%) | |
3 | 1 | reservoir | 425 (mM) | ||
4 | 1 | reservoir | Tris-Cl | 100 (mM) |