1C2B
ELECTROPHORUS ELECTRICUS ACETYLCHOLINESTERASE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 277 |
Detector technology | IMAGE PLATE |
Collection date | 1996-05-15 |
Detector | MARRESEARCH |
Spacegroup name | F 2 2 2 |
Unit cell lengths | 117.980, 215.870, 229.410 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 4.500 |
R-factor | 0.369 * |
Rwork | 0.369 |
R-free | 0.35100 |
Data reduction software | DENZO |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 10.000 |
High resolution limit [Å] | 4.500 |
Rmerge | 0.200 |
Total number of observations | 101833 * |
Number of reflections | 7742 |
Completeness [%] | 74.0 |
Redundancy | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8 | 20 * | NaKPO4, VAPOR DIFFUSION, pH 8.0, temperature 279K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium sulfate | 1.4 (M) |