1C12
INSIGHT IN ODORANT PERCEPTION: THE CRYSTAL STRUCTURE AND BINDING CHARACTERISTICS OF ANTIBODY FRAGMENTS DIRECTED AGAINST THE MUSK ODORANT TRASEOLIDE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Collection date | 1995-11-05 |
Detector | MARRESEARCH |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 40.400, 84.100, 134.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 12.000 - 2.600 |
R-factor | 0.205 |
Rwork | 0.205 |
R-free | 0.27000 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.650 * |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.700 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.130 | 0.300 |
Number of reflections | 15749 | |
<I/σ(I)> | 12 | |
Completeness [%] | 88.0 | 55 |
Redundancy | 5 | 1.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4 | 293 | drop solution was mixed with an equal volume of reservoir solution * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | hapten | 5 (mM) | |
2 | 1 | drop | Fab | 12 (mg/ml) | |
3 | 1 | drop | Tris-HCl | 100 (mM) | |
4 | 1 | reservoir | PEG8000 | 19 (%(w/v)) | |
5 | 1 | reservoir | sodium acetate | 75-200 (mM) |