1C0B
BOVINE PANCREATIC RIBONUCLEASE A DESICCATED FOR 2.5 DAYS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F1 |
Synchrotron site | CHESS |
Beamline | F1 |
Temperature [K] | 298 |
Detector technology | CCD |
Collection date | 1996-09-25 |
Detector | PRINCETON 2K |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 35.700, 39.700, 50.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.900 |
R-factor | 0.207 |
Rwork | 0.206 |
R-free | 0.27200 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.320 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MERLOT |
Refinement software | TNT (5E) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 9999.000 * | 2.100 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.060 | |
Total number of observations | 38053 * | |
Number of reflections | 5532 | |
<I/σ(I)> | 33.2 | |
Completeness [%] | 91.0 | 80 |
Redundancy | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | SMALL TUBES | 4.5 | 295 | 58% methanol (v/v), pH 4.5, SMALL TUBES, temperature 295K |