1BYL
BLEOMYCIN RESISTANCE PROTEIN FROM STREPTOALLOTEICHUS HINDUSTANUS
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | SIEMENS |
| Temperature [K] | 293 |
| Detector technology | AREA DETECTOR |
| Collection date | 1991-04-15 |
| Detector | SIEMENS |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 48.400, 48.400, 111.500 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.300 |
| R-factor | 0.176 |
| Rwork | 0.176 |
| Structure solution method | MIRAS |
| RMSD bond length | 0.015 |
| RMSD bond angle | 3.200 |
| Data reduction software | X-GEN |
| Data scaling software | X-GEN |
| Phasing software | PHASER |
| Refinement software | X-PLOR (2.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.500 | 2.440 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Rmerge | 0.067 * | |
| Total number of observations | 49546 * | |
| Number of reflections | 5959 | |
| <I/σ(I)> | 48.4 | 4.24 |
| Completeness [%] | 93.3 | 58 |
| Redundancy | 8.3 | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | other * | 6 | Rondeau, J.M., (1989) J. Mol. Biol., 207, 645. * |
