1BRA
RELOCATING A NEGATIVE CHARGE IN THE BINDING POCKET OF TRYPSIN
Experimental procedure
Spacegroup name | I 2 3 |
Unit cell lengths | 124.400, 124.400, 124.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.200 |
R-factor | 0.156 |
RMSD bond length | 0.012 |
RMSD bond angle | 3.200 |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.200 * |
Rmerge | 0.089 * |
Total number of observations | 50400 * |
Number of reflections | 18200 * |
Completeness [%] | 73.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8 * | 17 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | trypsin | 10 (mg/ml) | |
2 | 1 | reservoir | 25 (%) | ||
3 | 1 | reservoir | Tris-HCl | 40 (mM) | |
4 | 1 | reservoir | benzamidine | 75 (mM) |