1BQL

STRUCTURE OF AN ANTI-HEL FAB FRAGMENT COMPLEXED WITH BOBWHITE QUAIL LYSOZYME

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	54.800, 74.800, 79.000
Unit cell angles	90.00, 101.80, 90.00

Refinement procedure

Resolution	8.000 - 2.600
R-factor	0.191
Rwork	0.191
R-free	0.29100
RMSD bond length	0.009 *
RMSD bond angle	1.900 *
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.600 *
Rmerge	0.074 *
Total number of observations	30801 *
Number of reflections	15950 *
Completeness [%]	80.8 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	Fab	9.1 (mg/ml)
2	1	drop	BWQL	3.8 (mg/ml)
3	1	reservoir	PEG4000	14 (%)
4	1	reservoir	imidazole	0.1 (M)	pH7.0
5	1	reservoir	spermine	0.007 (%)