1BP3
THE XRAY STRUCTURE OF A GROWTH HORMONE-PROLACTIN RECEPTOR COMPLEX
Experimental procedure
| 実験手法 | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL7-1 |
| Synchrotron site | SSRL |
| Beamline | BL7-1 |
| Temperature [K] | 300 |
| Detector technology | IMAGE PLATE |
| Detector | MARRESEARCH |
| Spacegroup name | P 21 21 2 |
| 格子定数 [Å] | 154.200, 69.800, 43.300 |
| 格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
| 残基 | 10.000 - 2.900 |
| Rwork | 0.220 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1a22 |
| 結合長の平均二乗偏差(RMSD) [Å] | 0.019 |
| 結合角の平均二乗偏差(RMSD) [度] | 0.046 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | X-PLOR |
| Refinement software | PROLSQ |
Quality characteristics
| Overall | Outer shell | |
| 分解能 [Å] (低) | 10.000 | 3.000 |
| 分解能 [Å] (高) | 2.900 | 2.900 |
| Rmerge_l_obs | 0.108 | |
| 独立反射数 | 9883 | |
| 完全性 [%] | 93.0 | 89 |
結晶化条件
| 結晶ID | 方法 | pH | 温度 | 溶液条件 |
| 1 | 6 | pH 6.00 |
