1BOI
N-TERMINALLY TRUNCATED RHODANESE
Experimental procedure
Source type | ROTATING ANODE |
Source details | MACSCIENCE M18X |
Temperature [K] | 293 |
Detector technology | AREA DETECTOR |
Collection date | 1997-10 |
Detector | SIEMENS HI-STAR |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 90.690, 73.250, 39.670 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.000 - 2.200 |
R-factor | 0.162 |
Rwork | 0.162 |
R-free | 0.21900 |
RMSD bond length | 0.012 |
RMSD bond angle | 24.300 * |
Data reduction software | SAINT |
Data scaling software | SAINT |
Phasing software | X-PLOR (3.0) |
Refinement software | X-PLOR (3.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.000 | 2.300 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.104 | 0.190 |
Total number of observations | 109730 * | |
Number of reflections | 13716 * | |
Completeness [%] | 97.1 | 77.5 |
Redundancy | 8.1 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 7.3 | 4 * | pH 7.3 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 4 (mg/ml) | |
2 | 1 | drop | PEG6000 | 10 (%(w/v)) | |
3 | 1 | drop | Tris-HCl | 50 (mM) | |
4 | 1 | drop | sodium acetate | 50 (mM) | |
5 | 1 | drop | sodium thiosulfate | 1 (mM) | |
6 | 1 | reservoir | PEG6000 | 16 (%(w/v)) | |
7 | 1 | reservoir | Tris-HCl | 50 (mM) | |
8 | 1 | reservoir | sodium acetate | 50 (mM) | |
9 | 1 | reservoir | sodium thiosulfate | 1 (mM) |