1BOH
SULFUR-SUBSTITUTED RHODANESE (ORTHORHOMBIC FORM)
Experimental procedure
Temperature [K] | 297 |
Detector technology | AREA DETECTOR |
Collection date | 1997-10 |
Detector | SIEMENS |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 89.740, 72.350, 39.070 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.000 - 2.300 |
R-factor | 0.166 |
Rwork | 0.166 |
R-free | 0.21500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1rhs |
RMSD bond length | 0.013 |
RMSD bond angle | 24.600 * |
Data reduction software | XENGEN |
Data scaling software | SAINT |
Phasing software | AMoRE |
Refinement software | X-PLOR (3.83) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.000 | 2.420 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.110 | 0.340 |
Total number of observations | 60362 * | |
Number of reflections | 10362 | |
Completeness [%] | 78.8 | 13.4 |
Redundancy | 5.9 | 1.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 7.3 | 4 * | pH 7.3 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 4 (mg/ml) | |
2 | 1 | drop | PEG6000 | 10 (%(w/v)) | |
3 | 1 | drop | Tris-HCl | 50 (mM) | |
4 | 1 | drop | sodium acetate | 50 (mM) | |
5 | 1 | drop | sodium thiosulfate | 1 (mM) | |
6 | 1 | reservoir | PEG6000 | 16 (%(w/v)) | |
7 | 1 | reservoir | Tris-HCl | 50 (mM) | |
8 | 1 | reservoir | sodium acetate | 50 (mM) | |
9 | 1 | reservoir | sodium thiosulfate | 1 (mM) |