Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

1BNM

CARBONIC ANHYDRASE II INHIBITOR

Experimental procedure
Source typeROTATING ANODE
Source detailsRIGAKU RUH2R
Temperature [K]298
Detector technologyIMAGE PLATE
Collection date1995-07
DetectorRIGAKU RAXIS IIC
Spacegroup nameP 1 21 1
Unit cell lengths42.700, 41.700, 73.000
Unit cell angles90.00, 104.60, 90.00
Refinement procedure
Resolution6.500 - 2.600
R-factor0.137
Rwork0.137
Structure solution methodOTHER
Starting model (for MR)1CBA
RMSD bond length0.008
RMSD bond angle25.400

*

Data reduction softwareMOSFLM
Data scaling softwareCCP4
Phasing softwareX-PLOR (3.1)
Refinement softwareX-PLOR (3.1)
Data quality characteristics
 Overall
Low resolution limit [Å]6.500
High resolution limit [Å]2.600
Rmerge0.096
Total number of observations22271

*

Number of reflections7539
Completeness [%]96.4
Redundancy3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion, sitting drop

*

8

*

pH 10.0
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropenzyme6.7-7.4 (mg/ml)
21dropTris-HCl50 (mM)
31reservoirTris-HCl50 (mM)
41reservoirammonium sulfate1.75-2.50 (M)

217705

PDB entries from 2024-03-27

PDB statisticsPDBj update infoContact PDBjnumon