1BND
STRUCTURE OF THE BRAIN-DERIVED NEUROTROPHIC FACTOR(SLASH)NEUROTROPHIN 3 HETERODIMER
Experimental procedure
Detector technology | IMAGE PLATE |
Collection date | 1994-01-04 |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 98.400, 45.100, 68.000 |
Unit cell angles | 90.00, 118.30, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.300 |
R-factor | 0.182 |
Rwork | 0.182 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.890 |
Data reduction software | DENZO |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 * | |
High resolution limit [Å] | 2.300 * | 2.300 * |
Rmerge | 0.082 | 0.150 * |
Number of reflections | 11691 * | 1455 * |
Completeness [%] | 93.4 | 85.6 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 5.6 * | 18 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 15 (mg/ml) | |
2 | 1 | reservoir | PEG4000 | 10 (%(w/v)) | |
3 | 1 | reservoir | 2-propanol | 10 (%(v/v)) | |
4 | 1 | reservoir | sodium citrate | 0.1 (M) |