1BJ9

EFFECT OF UNNATURAL HEME SUBSTITUTION ON KINETICS OF ELECTRON TRANSFER IN CYTOCHROME C PEROXIDASE

Experimental procedure

Source type	ROTATING ANODE
Source details	RIGAKU RUH2R
Temperature [K]	273
Detector technology	AREA DETECTOR
Collection date	1997-06
Spacegroup name	P 21 21 21
Unit cell lengths	105.197, 74.364, 45.402
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 2.200
R-factor	0.179
RMSD bond length	0.010
RMSD bond angle	2.648
Refinement software	TNT (1)

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	2.200	2.200
Number of reflections	24668
<I/σ(I)>		2.2
Completeness [%]	98.0

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		6		pH 6