1BIL
CRYSTALLOGRAPHIC STUDIES ON THE BINDING MODES OF P2-P3 BUTANEDIAMIDE RENIN INHIBITORS
Experimental procedure
Spacegroup name | P 21 3 |
Unit cell lengths | 143.100, 143.100, 143.100 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.400 |
R-factor | 0.17 |
Rwork | 0.170 |
RMSD bond length | 0.017 |
RMSD bond angle | 2.700 |
Phasing software | X-PLOR |
Refinement software | TNT |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.400 * |
Rmerge | 0.063 * |
Number of reflections | 32160 * |
Completeness [%] | 90.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 4.5 * | 23 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 20 (mg/ml) | |
2 | 1 | reservoir | sodium citrate | 50 (mM) | |
3 | 1 | reservoir | 0.6 (M) | ||
4 | 1 | reservoir | PEG3350 | 10 (%(w/v)) |