1BH0
STRUCTURE OF A GLUCAGON ANALOG
Experimental procedure
| Source details | ENRAF-NONIUS |
| Temperature [K] | 287 |
| Detector technology | DIFFRACTOMETER |
| Collection date | 1985-06 |
| Detector | ENRAF-NONIUS FAST |
| Spacegroup name | P 21 3 |
| Unit cell lengths | 47.900, 47.900, 47.900 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 6.000 - 3.000 |
| Structure solution method | ISOMORPHOUS TO EXISTING NATIVE GLUCAGON STRUCTURE |
| RMSD bond length | 0.025 * |
| RMSD bond angle | 3.300 * |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 3.000 |
| Redundancy | 1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Batch method * | 9.24 * | 50 * | cooled down from 50degree * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | protein | 4.40mg | |
| 2 | 1 | 1 | phosphate | 0.2 (M) |
