1BGE
CRYSTAL STRUCTURE OF CANINE AND BOVINE GRANULOCYTE-COLONY STIMULATING FACTOR (G-CSF)
Experimental procedure
Spacegroup name | P 1 21 1 |
Unit cell lengths | 53.200, 35.900, 91.000 |
Unit cell angles | 90.00, 101.80, 90.00 |
Refinement procedure
Resolution | 7.000 - 2.200 |
R-factor | 0.193 |
Rwork | 0.193 |
RMSD bond length | 0.013 |
RMSD bond angle | 2.500 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.200 * |
Rmerge | 0.046 * |
Number of reflections | 15536 * |
Completeness [%] | 90.2 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6.54 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | canine G-CSF solution | 18.0 (mg/ml) | |
2 | 1 | drop | ethanol | 5.85 (%) | |
3 | 1 | drop | HEPES | 50 (mM) | adjusted to pH6.54 by NaOH |
4 | 1 | drop | ammonium sulfate | 255 (mM) | |
5 | 1 | reservoir | ethanol | 5.85 (%) | |
6 | 1 | reservoir | HEPES | 50 (mM) | adjusted to pH6.54 by NaOH |
7 | 1 | reservoir | ammonium sulfate | 255 (mM) |