1BGD
CRYSTAL STRUCTURE OF CANINE AND BOVINE GRANULOCYTE-COLONY STIMULATING FACTOR (G-CSF)
Experimental procedure
Spacegroup name | C 1 2 1 |
Unit cell lengths | 99.200, 36.200, 48.600 |
Unit cell angles | 90.00, 96.40, 90.00 |
Refinement procedure
Resolution | 7.000 - 2.300 |
R-factor | 0.207 |
Rwork | 0.207 |
RMSD bond length | 0.014 |
RMSD bond angle | 2.570 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 * |
High resolution limit [Å] | 2.300 * |
Rmerge | 0.044 * |
Total number of observations | 18417 * |
Number of reflections | 6830 * |
Completeness [%] | 88.2 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6.54 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | canine G-CSF solution | 22.8 (mg/ml) | |
2 | 1 | drop | ethanol | 5.80 (%(v/v)) | |
3 | 1 | drop | HEPES | 50 (mM) | adjusted to pH6.54 with NaOH |
4 | 1 | drop | ammonium sulfate | 200 (mM) | |
5 | 1 | reservoir | ethanol | 5.80 (%(v/v)) | |
6 | 1 | reservoir | HEPES | 50 (mM) | adjusted to pH6.54 with NaOH |
7 | 1 | reservoir | ammonium sulfate | 200 (mM) |