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1BEN

INSULIN COMPLEXED WITH 4-HYDROXYBENZAMIDE

Experimental procedure
Detector technologyIMAGE PLATE
Collection date1994-02-14
DetectorRIGAKU RAXIS IIC
Spacegroup nameH 3
Unit cell lengths80.720, 80.720, 37.630
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution8.000 - 1.400
R-factor0.154

*

RMSD bond length0.014
RMSD bond angle0.034
Refinement softwarePROFFT
Data quality characteristics
 Overall
Low resolution limit [Å]80.000
High resolution limit [Å]1.400
Rmerge0.066
Total number of observations159339

*

Number of reflections18002
Completeness [%]76.6
Redundancy8.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1unknown

*

5.70.05M SODIUM CITRATE, 0.007M ZINC ACETATE, 0.06M 4-HYDROXYBENZAMIDE, 1.0M SODIUM CHLORIDE, PH=5.7. CRYSTALS GROWN BY SLOW COOLING., slow cooling
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
111insulin0.9 (mM)
211sodium citrate0.05 (M)
311zinc acetate0.007 (M)
4114-hydroxybenzamide0.06 (M)
5111.0 (M)

217705

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