1BEN
INSULIN COMPLEXED WITH 4-HYDROXYBENZAMIDE
Experimental procedure
Detector technology | IMAGE PLATE |
Collection date | 1994-02-14 |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | H 3 |
Unit cell lengths | 80.720, 80.720, 37.630 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 1.400 |
R-factor | 0.154 * |
RMSD bond length | 0.014 |
RMSD bond angle | 0.034 |
Refinement software | PROFFT |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 80.000 |
High resolution limit [Å] | 1.400 |
Rmerge | 0.066 |
Total number of observations | 159339 * |
Number of reflections | 18002 |
Completeness [%] | 76.6 |
Redundancy | 8.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 5.7 | 0.05M SODIUM CITRATE, 0.007M ZINC ACETATE, 0.06M 4-HYDROXYBENZAMIDE, 1.0M SODIUM CHLORIDE, PH=5.7. CRYSTALS GROWN BY SLOW COOLING., slow cooling |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | insulin | 0.9 (mM) | |
2 | 1 | 1 | sodium citrate | 0.05 (M) | |
3 | 1 | 1 | zinc acetate | 0.007 (M) | |
4 | 1 | 1 | 4-hydroxybenzamide | 0.06 (M) | |
5 | 1 | 1 | 1.0 (M) |