1BE3
CYTOCHROME BC1 COMPLEX FROM BOVINE
Experimental procedure
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID2 |
Synchrotron site | ESRF |
Beamline | ID2 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1997-09 |
Detector | MARRESEARCH |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 211.200, 211.200, 339.280 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.000 - 3.000 |
Rwork | 0.260 |
R-free | 0.32000 |
Structure solution method | MIR |
RMSD bond length | 0.010 |
RMSD bond angle | 0.032 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CCP4 |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 3.110 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.070 | 0.266 |
Total number of observations | 223182 * | |
Number of reflections | 79396 | |
<I/σ(I)> | 12.6 | 2.6 |
Completeness [%] | 88.9 | 76.8 |
Redundancy | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 6.6 | pH 6.6 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | n-dodecyl-beta-D-maltoside | 0.015 (%) | |
2 | 1 | 1 | 100 (mM) | ||
3 | 1 | 1 | PEG4000 | 6-8 (%) |