1BDV
ARC FV10 COCRYSTAL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 200 |
Detector technology | IMAGE PLATE |
Collection date | 1996-11-15 |
Detector | RIGAKU RAXIS II |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 62.840, 56.310, 52.980 |
Unit cell angles | 90.00, 105.03, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.800 |
R-factor | 0.252 * |
Rwork | 0.243 |
R-free | 0.29700 * |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1par |
RMSD bond length | 0.010 * |
RMSD bond angle | 1.573 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.590 |
High resolution limit [Å] | 2.800 | 2.500 |
Rmerge | 0.081 | |
Number of reflections | 8691 | |
<I/σ(I)> | 2 | |
Completeness [%] | 97.5 | 62 |
Redundancy | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8 * | pH 6.5 |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | PEG 400 | ||
2 | 1 | 1 | GLYCEROL | ||
3 | 1 | 1 | CACODYLATE | ||
4 | 1 | 1 | MGCL2 | ||
5 | 1 | 1 | COBALTHEXAMMINE |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 15 (mg/ml) | |
2 | 1 | reservoir | ammonium phosphate | 55 (%sat) |