1BCS
COMPLEX OF THE WHEAT SERINE CARBOXYPEPTIDASE, CPDW-II, WITH THE MICROBIAL PEPTIDE ALDEHYDE INHIBITOR, CHYMOSTATIN, AND ARGININE AT 100 DEGREES KELVIN
Experimental procedure
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 95.400, 95.400, 208.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.000 - 2.100 * |
R-factor | 0.174 |
RMSD bond length | 0.016 |
RMSD bond angle | 2.800 * |
Data reduction software | R-AXIS |
Refinement software | TNT |
Data quality characteristics
Overall | Outer shell | |
High resolution limit [Å] | 2.100 * | 2.100 * |
Rmerge | 0.040 | |
Total number of observations | 127152 * | |
Number of reflections | 46630 * | |
Completeness [%] | 81.0 * | 23 * |
Redundancy | 2.75 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | 100 (mM) | ||
2 | 1 | drop | PEG4000 | 0.2 (%(w/v)) | |
3 | 1 | reservoir | sodium chloride | 1.25 (M) | |
4 | 1 | reservoir | sodium acetate | 50 (mM) | |
5 | 1 | drop | sodium acetate | 50 (mM) |