1BCR
COMPLEX OF THE WHEAT SERINE CARBOXYPEPTIDASE, CPDW-II, WITH THE MICROBIAL PEPTIDE ALDEHYDE INHIBITOR, ANTIPAIN, AND ARGININE AT ROOM TEMPERATURE
Experimental procedure
Temperature [K] | 290 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 98.400, 98.400, 209.500 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 21.000 - 2.500 |
R-factor | 0.162 |
RMSD bond length | 0.016 |
RMSD bond angle | 2.530 |
Data reduction software | R-AXIS |
Refinement software | TNT |
Data quality characteristics
Overall | Outer shell | |
High resolution limit [Å] | 2.500 * | 2.500 * |
Rmerge | 0.054 | |
Total number of observations | 65638 * | |
Number of reflections | 29444 * | |
Completeness [%] | 86.0 * | 71 * |
Redundancy | 2.23 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | 100 (mM) | ||
2 | 1 | drop | PEG4000 | 0.2 (%(w/v)) | |
3 | 1 | drop | sodium acetate | 50 (mM) | |
4 | 1 | reservoir | sodium chloride | 1.25 (M) | |
5 | 1 | reservoir | sodium acetate | 50 (mM) |