1BAB

HEMOGLOBIN THIONVILLE: AN ALPHA-CHAIN VARIANT WITH A SUBSTITUTION OF A GLUTAMATE FOR VALINE AT NA-1 AND HAVING AN ACETYLATED METHIONINE NH2 TERMINUS

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	63.200, 83.600, 53.800
Unit cell angles	90.00, 99.30, 90.00

Refinement procedure

Resolution	? - 1.500
R-factor	0.157
RMSD bond length	0.016
RMSD bond angle	0.031
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	1.590 *
Rmerge	0.054 *
Total number of observations	754736 *
Number of reflections	69608 *
Completeness [%]	93.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	6.5 *		Perutz, M.F., (1968) J. Cryst. Growth, 2, 54. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	ammonium sulfate	4 (M)
2	1	1		2 (M)
3	1	1		2 (M)