1B9W

C-TERMINAL MEROZOITE SURFACE PROTEIN 1 FROM PLASMODIUM CYNOMOLGI

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	LURE BEAMLINE DW32
Synchrotron site	LURE
Beamline	DW32
Temperature [K]	293
Detector technology	IMAGE PLATE
Collection date	1998-03
Detector	MARRESEARCH
Spacegroup name	P 32 2 1
Unit cell lengths	43.770, 43.770, 92.040
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	15.000 - 1.800
R-factor	0.212 *
Rwork	0.212
R-free	0.27900
Structure solution method	SIRAS
RMSD bond length	0.015
RMSD bond angle	0.026
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	SHARP
Refinement software	REFMAC

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	15.000
High resolution limit [Å]	1.800
Rmerge	0.058 *	0.338 *
Number of reflections	9965
Completeness [%]	100.0
Redundancy	13.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	5.6 *		pH 5.50

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	PEG4000	30 (%(w/v))
2	1	1	ammonium acetate	0.2 (M)
3	1	1	sodium citrate	0.1 (M)