1B9L
7,8-DIHYDRONEOPTERIN TRIPHOSPHATE EPIMERASE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Temperature [K] | 287 |
Spacegroup name | P 41 |
Unit cell lengths | 69.680, 69.680, 239.720 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.900 |
Rwork | 0.188 |
R-free | 0.25900 |
Structure solution method | MIR |
RMSD bond length | 0.010 |
RMSD bond angle | 2.055 |
Refinement software | X-PLOR (3.8) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.900 |
Rmerge | 0.119 |
Total number of observations | 68471 * |
Number of reflections | 23361 |
Completeness [%] | 94.6 |
Redundancy | 2.93 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 7 | 20 * | pH 7.0 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ethylene glycol | 35 (%) |