1B9L
7,8-DIHYDRONEOPTERIN TRIPHOSPHATE EPIMERASE
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Temperature [K] | 287 |
| Spacegroup name | P 41 |
| Unit cell lengths | 69.680, 69.680, 239.720 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.900 |
| Rwork | 0.188 |
| R-free | 0.25900 |
| Structure solution method | MIR |
| RMSD bond length | 0.010 |
| RMSD bond angle | 2.055 |
| Refinement software | X-PLOR (3.8) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.900 |
| Rmerge | 0.119 |
| Total number of observations | 68471 * |
| Number of reflections | 23361 |
| Completeness [%] | 94.6 |
| Redundancy | 2.93 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, sitting drop * | 7 | 20 * | pH 7.0 |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | ethylene glycol | 35 (%) |
