1B71
RUBRERYTHRIN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Temperature [K] | 298 |
Detector technology | AREA DETECTOR |
Detector | XUONG-HAMLIN MULTIWIRE |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 49.300, 81.300, 100.100 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.900 |
R-factor | 0.195 |
Structure solution method | OTHER |
Starting model (for MR) | PDB IDENTIFIER 1RYT |
RMSD bond length | 0.006 |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 1.900 |
Rmerge | 0.093 |
Number of reflections | 15420 |
<I/σ(I)> | 9.4 |
Completeness [%] | 94.8 |
Redundancy | 15.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8 | pH 8 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | TRIZMA hydrochloride | 0.1 (M) | |
2 | 1 | reservoir | PEG1450 | 15 (%) |