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1B26

GLUTAMATE DEHYDROGENASE

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsMACSCIENCE
Temperature [K]286
Detector technologyIMAGE PLATE
DetectorMARRESEARCH
Spacegroup nameP 31 2 1
Unit cell lengths147.130, 147.130, 273.640
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution8.000 - 3.000
Rwork0.225
R-free0.29500
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.006
RMSD bond angle21.140

*

Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareX-PLOR
Refinement softwareX-PLOR (3.8)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0003.100
High resolution limit [Å]3.0003.000
Rmerge0.091
Total number of observations220980

*

Number of reflections57305
Completeness [%]94.075
Redundancy3.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1unknown

*

6.5CRYSTALLIZATION CONDITIONS: 3% POLYETHYLENE GLYCOLE, 120 MM AMMONIUM ACETATE 50 MM BIS-TRIS PROPANE PH 6.5
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
111PEG3 (%)
211ammonium acetate120 (mM)
311Bis-Tris propane50 (mM)

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PDB entries from 2024-03-27

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