1B06
SUPEROXIDE DISMUTASE FROM SULFOLOBUS ACIDOCALDARIUS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 286 |
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 168.100, 91.300, 85.700 |
Unit cell angles | 90.00, 91.40, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.200 |
R-factor | 0.174 |
Rwork | 0.174 |
R-free | 0.22300 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 24.360 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | X-PLOR (3.8) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | |
High resolution limit [Å] | 2.200 | 2.200 * |
Rmerge | 0.101 | |
Total number of observations | 248523 * | |
Number of reflections | 69271 | |
Completeness [%] | 99.5 * | 95 * |
Redundancy | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 7.5 | 20 * | pH 7.5 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG4000 | 16.25 (%) | |
2 | 1 | reservoir | ammonium sulfate | 0.2 (M) | |
3 | 1 | reservoir | 2-propanol | 5 (%(w/v)) | |
4 | 1 | reservoir | HEPES | 0.1 (M) |