1AZB

STRUCTURE OF APO-AZURIN FROM ALCALIGENES DENITRIFICANS AT 1.8 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	C 2 2 21
Unit cell lengths	75.100, 74.300, 99.000
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 2.200
R-factor	0.158
RMSD bond length	0.013
RMSD bond angle	0.047 *
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	2.200 *
Rmerge	0.050 *
Number of reflections	16203 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	interface diffusion *	6 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	phosphate	0.1 (M)
2	1	1	ammonium sulphate	40 (%sat)
3	1	1	protein	14 (mg/ml)
4	1	2	ammonium sulfate	80 (%sat)