1AYB
CRYSTAL STRUCTURES OF PEPTIDE COMPLEXES OF THE AMINO-TERMINAL SH2 DOMAIN OF THE SYP TYROSINE PHOSPHATASE
Experimental procedure
Spacegroup name | P 43 21 2 |
Unit cell lengths | 62.900, 62.900, 77.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 3.000 |
R-factor | 0.164 |
Rwork | 0.164 |
RMSD bond length | 0.014 |
RMSD bond angle | 3.000 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 * |
High resolution limit [Å] | 3.000 * |
Rmerge | 0.089 * |
Number of reflections | 2549 * |
Completeness [%] | 73.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6 * | 4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | IRS1-895 peptide | ||
2 | 1 | reservoir | PEG monomethyl ether 2000 | 25 (%) | |
3 | 1 | reservoir | MES | 100 (mM) | |
4 | 1 | reservoir | ammonium sulfate | 50 (mM) | |
5 | 1 | reservoir | protein |