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1AW9

STRUCTURE OF GLUTATHIONE S-TRANSFERASE III IN APO FORM

Experimental procedure
Source typeROTATING ANODE
Source detailsRIGAKU RUH2R
Temperature [K]290
Detector technologyIMAGE PLATE
Collection date1995-03
DetectorMARRESEARCH
Spacegroup nameP 63 2 2
Unit cell lengths97.770, 97.770, 116.450
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution8.000 - 2.200
R-factor0.197
Rwork0.197
R-free0.22400

*

RMSD bond length0.014
RMSD bond angle22.800

*

Data reduction softwareCCP4
Refinement softwareX-PLOR
Data quality characteristics
 OverallOuter shell
High resolution limit [Å]2.200

*

1.970
Rmerge0.087
Number of reflections15788
Completeness [%]99.5
Redundancy9.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion, hanging drop

*

7

*

pH 7.5
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein25 (mg/ml)
21dropHEPES10 (mM)pH7.0
31dropsodium azide0.02 (%)
41reservoir70 (mM)
51reservoirsodium acetate1.0 (M)
61reservoirHEPES0.1 (M)pH7.5
71reservoirsodium azide0.02 (%)

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