1AUN
PATHOGENESIS-RELATED PROTEIN 5D FROM NICOTIANA TABACUM
Experimental procedure
| Source type | ROTATING ANODE |
| Source details | RIGAKU RUH3R |
| Temperature [K] | 293 |
| Detector technology | IMAGE PLATE |
| Collection date | 1995-11 |
| Detector | RIGAKU |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 80.140, 63.690, 45.610 |
| Unit cell angles | 90.00, 107.18, 90.00 |
Refinement procedure
| Resolution | 10.000 - 1.800 |
| R-factor | 0.169 |
| Rwork | 0.169 |
| R-free | 0.21900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1thv |
| RMSD bond length | 0.007 |
| RMSD bond angle | 25.700 * |
| Data reduction software | PROCESS |
| Data scaling software | PROCESS |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 1.700 | |
| High resolution limit [Å] | 1.610 | 1.610 |
| Rmerge | 0.079 | 0.267 |
| Number of reflections | 21635 | |
| <I/σ(I)> | 11 | 2 |
| Completeness [%] | 75.3 | 31 |
| Redundancy | 3.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | other * | 7.5 | Koiwa, H., (1997) Plant Cell Physiol., 38, 783. * |
