1AQ2
PHOSPHOENOLPYRUVATE CARBOXYKINASE
Experimental procedure
Source details | ENRAF-NONIUS |
Temperature [K] | 300 |
Detector technology | DIFFRACTOMETER |
Collection date | 1996-10-15 |
Detector | ENRAF-NONIUS FAST |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 126.190, 96.610, 46.860 |
Unit cell angles | 90.00, 95.80, 90.00 |
Refinement procedure
Resolution | 6.000 - 1.900 |
R-factor | 0.218 |
Rwork | 0.218 |
R-free | 0.26000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ayl |
RMSD bond length | 0.007 |
RMSD bond angle | 1.320 |
Data reduction software | MADNES |
Data scaling software | CCP4 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.000 | 3.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 39324 | |
<I/σ(I)> | 4.3 | 2.1 |
Completeness [%] | 90.0 | 85 |
Redundancy | 2.6 | 2.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.4 | pH 4.4 |