1AOC
JAPANESE HORSESHOE CRAB COAGULOGEN
Experimental procedure
Source type | SYNCHROTRON |
Source details | MPG/DESY, HAMBURG BEAMLINE BW6 |
Synchrotron site | MPG/DESY, HAMBURG |
Beamline | BW6 |
Temperature [K] | 290 |
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 52.200, 52.200, 232.200 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 6.000 - 2.000 |
R-factor | 0.191 |
Rwork | 0.191 |
R-free | 0.28200 |
Structure solution method | MIRAS |
RMSD bond length | 0.011 |
RMSD bond angle | 2.150 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 |
Phasing software | X-PLOR (3.851) |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 2.070 | |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.046 | 0.187 |
Number of reflections | 23437 | |
Completeness [%] | 95.1 | 92.3 |
Redundancy | 1.8 | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 4.5 | 20 * | 0.5 M AMMONIUM SULFATE, 0.1 M NA-ACETATE, PH 4.5 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | coagulogen | 5.8-7 (mg/ml) | |
2 | 1 | drop | ammonium sulfate | 0.2 (M) | |
3 | 1 | drop | sodium acetate | 0.04 (M) | |
4 | 1 | drop | cadmium sulfate | 0.04 (mM) | |
5 | 1 | reservoir | ammonium sulfate | 0.5 (M) | |
6 | 1 | reservoir | sodium acetate | 0.1 (M) | |
7 | 1 | reservoir | cadmium sulfate | 0.1 (mM) |