1AO3
A3 DOMAIN OF VON WILLEBRAND FACTOR
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 287 |
Detector technology | IMAGE PLATE |
Collection date | 1993-11 |
Detector | RIGAKU |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 58.000, 65.100, 57.800 |
Unit cell angles | 90.00, 101.90, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.200 |
R-factor | 0.158 |
Rwork | 0.158 |
R-free | 0.21500 |
Structure solution method | MIR |
RMSD bond length | 0.010 |
RMSD bond angle | 26.000 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 8.000 | 2.300 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.056 * | |
Number of reflections | 15112 * | |
<I/σ(I)> | 11.1 | 4 |
Completeness [%] | 95.5 | 93.3 |
Redundancy | 2.1 | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8.5 | 22 * | 0.1M TRIS PH 8.5, 200MM MGCL2, 24% PEG 8K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG8000 | 24-32 (%) | |
2 | 1 | reservoir | Tris | 100 (mM) | |
3 | 1 | reservoir | 200 (mM) |