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1AN4

STRUCTURE AND FUNCTION OF THE B/HLH/Z DOMAIN OF USF

Experimental procedure
Source typeSYNCHROTRON
Source detailsCHESS BEAMLINE F1
Synchrotron siteCHESS
BeamlineF1
Temperature [K]253
Detector technologyIMAGE PLATE
Collection date1993-06-01
Spacegroup nameP 21 21 21
Unit cell lengths136.600, 54.700, 44.400
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution6.000 - 2.900
Rwork0.236
RMSD bond length0.019
RMSD bond angle3.050

*

Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareX-PLOR
Refinement softwareX-PLOR (3.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]15.0003.000
High resolution limit [Å]2.9002.900
Rmerge0.076
Total number of observations32049

*

Number of reflections6038
<I/σ(I)>14.4
Completeness [%]76.4

*

49.3
Redundancy2.61.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.5

*

4

*

pH 4.75, VAPOR DIFFUSION, HANGING DROP, temperature 277.00K
Crystallization Reagents
IDcrystal IDsolution IDreagent nameconcentrationdetails
111WATER
1012GLYCEROL
1112KCL
1212MGCL2
1312CD ACETATE
1412NA ACETATE
211PEG 400
311GLYCEROL
411KCL
511MGCL2
611CD ACETATE
711NA ACETATE
812WATER
912PEG 400
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropDNA1.4 (mM)
21drop100 (mM)
31dropHEPES10 (mM)
41reservoirPEG40015 (%)
51reservoirglycerol15 (%)
61reservoir100 (mM)
71reservoir2.8 (mM)
81reservoirCd(II) acetate1.4 (mM)
91reservoirsodium acetate100 (mM)

217705

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