1AL6
CHICKEN CITRATE SYNTHASE COMPLEX WITH N-HYDROXYAMIDO-COA AND OXALOACETATE
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 295 |
Detector technology | AREA DETECTOR |
Collection date | 1997-02-10 |
Detector | XUONG-HAMLIN MULTIWIRE |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 104.430, 78.480, 58.450 |
Unit cell angles | 90.00, 78.89, 90.00 |
Refinement procedure
Resolution | 25.000 - 1.850 |
Rwork | 0.157 |
Structure solution method | MOLECULAR SUBSTITUTION |
Starting model (for MR) | 1csh |
RMSD bond length | 0.014 |
RMSD bond angle | 2.200 |
Data reduction software | SDMS |
Data scaling software | SDMS |
Phasing software | TNT |
Refinement software | TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.000 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.047 | 0.155 |
Number of reflections | 34332 | |
<I/σ(I)> | 9.2 | 2.3 |
Completeness [%] | 87.0 | 78 |
Redundancy | 1.7 | 1.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | CRYSTALLIZED FROM 1.02M NA CITRATE, PH 6.0 5 MM OXALOACETATE, PH 6 2 MM N-HYDROXYAMIDOCARBOXYMETHYLDETHIA COENZYME A. |